A kind of discharging mechanism and discharging method of energy level molecular material cell tear equipment
Technical field
The present invention relates to field of nano material preparation, more particularly to a kind of discharging of energy level molecular material cell tear equipment
Mechanism and discharging method.
Background technology
At present, the preparation method and equipment of nano material mainly has following several:
1) high-pressure homogenization:Equipment is high pressure homogenizer, and it is constituted by between high-pressure pump and homogenate, ADV companies of Britain and U.S.
Microfluidics companies of state have product to sell.Its Cracking Mechanism:Molecular cell experienced during a series of to be made at a high speed
Into scissors, collision and by the change of high pressure to normal pressure so as to cause molecular cell crush.The problem of presence is:It is easier to make
Into the bulk or filamentous fungi molecular cell of blocking, less Gram-positive is first and some submolecule cells, and quality is hard,
Easy damaged is homogenized valve, is also not suitable for being processed with the method.
2) high speed bead mill method:Equipment is ball mill, and WBC companies of Switzerland and Mechanology Inc. of Siemens manufacture various types
Number ball mill, under its disintegrating machine:Microbial cell suspension is sufficiently mixed with superfine grinding agent under stirring slurry effect, pearl
Shear, collide with mutual between son and between pearl and molecular cell, promoting molecular cell wall to crush, disengaging inclusion,
Under the assistance of pearl wave separator, pearl is trapped in broken interior, and slurries flow out, and so as to realize continuous operation, in crushing, produces
Heat taken away by the coolant in chuck.The problem of presence is:Operating parameter is more, typically estimates by rule of thumb and between pearl
Loss of liquid 30% or so.
3) ultrasonication:It is thin that ultrasonic wave of the frequency higher than 15~20KHz can carry out molecule in the case where high sound intensity can be input into
Born of the same parents crush.Its Cracking Mechanism:The shock wave and shearing force that may cause with cavitation phenomenon is relevant.The efficiency and sound of ultrasonication
Frequently, the factor such as acoustic energy, process time, molecular cell concentration and first type is relevant.Existing problems are;Ultrasonic disruption is in experiment
Room sizable application is more universal, processes easy to operate during a small amount of sample, and liquid measure loss is few, but the chemical free-radical that ultrasonic wave is produced
Group can make some Sensitive active substances deactivations.And Large Copacity device acoustic energy is transmitted, radiating is had any problem.
4) the micro-nano broken wall of low temperature:Material is placed in a low temperature of -170 degree freezes it, subsequently melts at normal temperatures, such as
This is repeatedly so that molecular cell wall is crushed.The problem of presence:Build low temperature environment higher to device requirement, it is broken using the temperature difference
It is relatively costly.
5) the molten method of enzyme:It is exactly the method for being dissolved cell membrane and cell membrane digestion with biology enzyme.Conventional lyase has bacteriolyze
Enzyme β -1.3- dextranases, protease etc..The problem of presence is;Product inhibition is easily caused, this is probably to cause intracellular thing
A low key factor of matter release rate.And lyase price is high, extensive utilization is limited.If reclaiming lyase, increase again
Hundred operations for isolating and purifying lyase.The molten method poor universality of other enzyme, different strain need to select different enzymes.
6) chemical osmosis:Some organic solvent (such as benzene, toluene), antibiotic, surfactant, metal-chelator, changes
The chemicals such as property agent can change the permeability of molecular cell wall or film so that inner mixture is selectively infiltrated.Its
The mechanism of action;Chemosmosis depends on the type of chemical reagent and the structure of molecular cell wall and film and composition.What is existed asks
Topic;Time is long, and efficiency is low;Chemical reagent toxicity is stronger, while to product also toxic effect, needing when further separating with thoroughly
The methods such as analysis remove these reagents;Poor universality:Certain reagent can only act on some certain types of microbial cells.
7) induced with laser method:Be allowed to gasify by the certain mode of heatings of block Jing, then it is condensed and formed Ultramicro-powder
Body is deposited and obtained.Single metal material can be produced according to above-mentioned process.The problem of presence;Synthetic quantity is little, it is little to be only capable of
Amount production, hourly output only has hectogram or so, cost intensive and changes many structures and property of material, and material phase
Change define its application.
For problems of the prior art, the applicant devises one kind, and " tear of energy level molecular material cell sets
It is standby ", according to Crow section theorem, required swirling turbulence fluid is formed using supersonic flow, torn using swirling turbulence fluid
Molecular material cell is split, so that the nano material of predetermined particle diameter is obtained.
The content of the invention
It is an object of the invention to provide a kind of uniform cell of constant discharging tears equipment discharging mechanism.
To reach object above, the present invention is adopted the following technical scheme that.
A kind of energy level molecular material cell tears the discharging mechanism of equipment, it is characterised in that include:Baffle plate, through baffle plate
At least one material outlet, and be arranged at least two negative-feedback pressure around material outlet and adjust mouth.
Used as with improvement, the cell tear equipment includes:Power plant module, feed module, energy field generator module, energy
Amount field chamber module and temperature exchange module;The energy field generator module is arranged in the module of energy field chamber, the charging mould
The inner space of block and energy field chamber module, the power plant module provides power for energy field generator module, and the temperature is handed over
The temperature of mold changing block control energy field chamber module, the baffle plate is arranged on the material outlet side of energy field chamber module.
Used as with improvement, the feed module includes:Funnel, the feeding conveyor structure below funnel, Yi Jishe
Put the airflow hole in the feed module left and right sides.
Used as with improvement, the charging structure for conveying includes:Motor, gear, transmission mechanism and screw conveyor shaft, institute
State motor and torque is passed to into gear, then transmission mechanism is exported by gear, and then drive screw conveyor shaft rotation.
Used as with improvement, the feed module is simultaneously the rear end bearing seat of the rotary shaft of energy field generator module, should
Rear end bearing seat is also connected with the side of temperature exchange module, and energy field chamber module clip is also handed in rear end bearing seat with temperature
Between mold changing block.
Used as with improvement, the energy field generator module includes:Circular leaf dish with rotary shaft and be fixed on leaf dish week
The stripping fork on edge, one end of the rotary shaft is connected by shaft coupling with motor output shaft, the other end of rotary shaft by bearing with
Material discharging module connects.
Used as with improvement, energy field chamber module is circular hollow cavity, is provided with the outer shroud of circular hollow cavity
Formula materials inlet, in the outer shroud lower end of circular hollow cavity cleaning solution outlet is provided with.
As the switch tooth bar with improvement, being provided with cleaning solution outlet for controlling its aperture, the switch tooth bar
Pass sequentially through the connection of gear train, gear train adjusting rod, gear train and adjustment disk.
Used as with improvement, the discharging mechanism is simultaneously the front end bearing block of the rotary shaft of energy field generator module, should
Front end bearing block is fixed on the center position of circular hollow cavity and constitutes a front cover in energy field chamber;The material outlet
It is arranged on along the plate body that edge of front end bearing block week extends out.
As with improvement, Material pipeline joint is additionally provided with discharging mechanism.
The present invention also provides a kind of discharging method based on above-mentioned discharging mechanism, it is characterised in that in energy field chamber, profit
With the effect of centrifugal force and centripetal force, make the big material of quality that the edge in energy field chamber is thrown by centrifugal force;And the little thing of quality
Under differential pressure action, centripetal force is allowed to gather energy field chamber centre material, and then draws collection by material outlet, realizes
Material without sieve separation.
As with improvement, while discharging, adjust toward negative-feedback pressure and inject simultaneously in mouth feedback air pressure, the feedback
Air pressure is drawn together in company with material from material outlet.
The invention has the beneficial effects as follows:During real work, by baffle plate setting on the energy field chamber that cell tears equipment, fill
When a side in energy field chamber, in energy field chamber, using the effect of centrifugal force and centripetal force, make the big material of quality by from
Mental and physical efforts throw the edge in energy field chamber;And the little material of quality, under differential pressure action, centripetal force is allowed to gather in energy field chamber
Center portion position, so by material outlet draw collect, realize material without sieve separation.Especially, draw material when, by
Inject feedback air pressure on negative-feedback pressure regulation mouth simultaneously and stablizing and uniform for material extraction is effectively ensured.
Description of the drawings
Fig. 1 show discharging mechanism structure principle chart;
Fig. 2 show cell tear device structure schematic diagram;
Fig. 3 show feed module structural representation;
Fig. 4 show feed module left view;
Fig. 5 show feed module right view;
Fig. 6 show power generator modular structure schematic diagram;
Fig. 7 show energy field chamber modular structure schematic diagram;
Fig. 8 show discharging mechanism structural representation.
Description of reference numerals:
1st, baffle plate, 2, material outlet, 3, negative-feedback pressure adjust mouth, 4, power plant module, 5, feed module, 6, energy field
Generator module, 7, energy field chamber module, 8, temperature exchange module, 9, Material pipeline joint;
51st, funnel, 52, feeding conveyor structure, 53,54,55, airflow hole;
61st, leaf dish, 62, stripping fork, 63, rotary shaft;
71st, formula materials inlet, 72, cleaning solution outlet, 73, switch tooth bar, 74, gear train, 75, adjusting rod, 76,
Gear train, 77, adjustment disk, 78, regulation handle.
Specific embodiment
For convenience of the essence that those skilled in the art more fully understand the present invention, below in conjunction with the accompanying drawings to the concrete of the present invention
Embodiment is described in detail.
As shown in figure 1, a kind of energy level molecular material cell tears the discharging mechanism of equipment, including:Baffle plate 1, through baffle plate 1
At least one material outlet 2, and be arranged at least two negative-feedback pressure around material outlet 2 and adjust mouth 3.
Concrete operating principle is:Baffle plate 1 is arranged on the energy field chamber of cell tear equipment, serves as the one of energy field chamber
Individual side, in energy field chamber, using the effect of centrifugal force and centripetal force, the material for making quality big throws energy field by centrifugal force
The edge in chamber;And the little material of quality, under differential pressure action, centripetal force is allowed to gather energy field chamber centre, and then by thing
Material outlet 2 draw collect, realize material without sieve separation.Especially, when material is drawn, by adjusting in negative-feedback pressure
Inject feedback air pressure on mouth 3 simultaneously and stablizing and uniform for material extraction is effectively ensured.
As shown in Fig. 2 the cell tear equipment includes:Power plant module 4, feed module 5, energy field generator module 6,
Energy field chamber module 7 and temperature exchange module 8.The energy field generator module 6 is arranged in energy field chamber module 7, is used for
One or more whirlpool of different-energy rank is produced in module 7 in energy field chamber, and then forms multilevel energy field, centrifugation
Power, centripetal force etc..The inner space of the feed module 5 and energy field chamber module 7, is that energy field chamber module 7 provides to be comminuted
Material.The power plant module 4 is that energy field generator module 6 provides power, and the temperature exchange module 8 is used for controlling energy field
The operating temperature of chamber module 7, the baffle plate is arranged on the material outlet side of energy field chamber module 7.
As shown in Figure 3-Figure 5, the feed module 5 includes:Funnel 51, installed in the feeding conveyor structure of the lower section of funnel 51
52, and it is arranged on airflow hole 53, airflow hole 54 and the airflow hole 55 of the feed module left and right sides.The charging structure for conveying bag
Include:Motor, gear, transmission mechanism and screw conveyor shaft.During production, torque is passed to gear by motor, then by becoming
Fast mechanism exports transmission mechanism, and then drives screw conveyor shaft rotation, reaches the purpose of material conveying.Need injection air-flow by
Airflow hole 54,55 plays regulation through the arrival energy field cavity of airflow hole 53, and its is acted on.During cleaning, cleaning agent by airflow hole 54,
55 reach energy field cavity through airflow hole 53 plays cleaning action;Equally, hot-air also can be by airflow hole 54,55 through air-flow
Hole 53 reaches energy field cavity and plays desiccation.
Especially, feed module 5 is simultaneously the rear end bearing seat of the rotary shaft of energy field generator module, the rear end bearing
Seat is also connected with the side of temperature exchange module 8, by energy field generator module and energy field chamber module clip therebetween.
As shown in fig. 6, the energy field generator module 6 includes:With rotation 63 leaf dish 61 and be fixed on leaf dish 61 weeks
The stripping fork 62 on edge.In the present embodiment, preferred power plant module 4 is motor.During concrete installation, one end of the rotary shaft 63 of leaf dish 61 passes through
Shaft coupling is connected with motor output shaft, and the other end is connected by bearing with material discharging module.
As shown in fig. 7, energy field chamber module 7 is circular hollow cavity, it is provided with the outer shroud of circular hollow cavity
Formula materials inlet 71, in the outer shroud lower end of circular hollow cavity cleaning solution outlet 72 is provided with.The cleaning solution outlet
72 control aperture by switching tooth bar 73.Specifically, the switch tooth bar 73 passes sequentially through gear train 74, gear train adjusting rod
75th, gear train 76, adjustment disk 77 are connected with regulation handle 78.During real work, by manipulating regulation handle 78 control is can reach
The purpose of the aperture of cleaning solution outlet 72 processed.In other embodiments, the gear train adjusting rod 75, gear train 76, regulation
Disk 77 is replaced with regulation handle 78 using electric structure;To improve turbulence effects, at the edge of circular hollow cavity rule are additionally provided with
Then and/or irregular tooth-shape structure;It is not limited to the present embodiment.
As shown in figure 8, the discharging mechanism is simultaneously the front end bearing block of the rotary shaft of energy field generator module 6, should
Front end bearing block is fixed on the center position of circular hollow cavity and constitutes a front cover in energy field chamber.Material outlet 2 sets
Put in front end bearing block week along the plate body for extending out, negative-feedback pressure adjusts mouth (not shown) and is arranged on material outlet
Around.For convenience of the collection of material, Material pipeline joint 9 is additionally provided with discharging mechanism.
Compared with prior art, the energy level molecular material cell tear equipment that the present embodiment is provided, can manufacture as needed
The molecular material of variety classes and particle diameter, by power plant module guide energy field generator module different-energy rank one is produced
Individual or multiple whirlpools form multilevel energy field so that material differential work of energy in one or more height swirling turbulence
With the wind tunnel effect for forming different stage, moment crushes the tear of molecular material cell, in the random pulse of swirling turbulence body
In the shock wave of the different-energy rank produced with wind tunnel effect, molecular material cell in multiple complicated high speed mechanicses collisions,
And infiltration and counter-infiltration of the energy inside and outside molecular material cell membrane and cell membrane repeatedly, macromolecular material particle is due to wind-tunnel
Tear ring cavity swirling turbulence turbine is constantly thrown in the effect of effect, swirling turbulence body random pulse and centrifugal force etc.
Periphery, is all torn again crushing in swirling turbulence body, including implosion and splits outward.Setting reaches required molecular material particle
Small powder under diameter (1 nanometer to 10 microns) yardstick is re-introduced into the centre bit of swirling turbulence turbine, by energy level molecule material
Expect that cell tears the controller of equipment discharging opening and draws and be recovered (straight according to the particle for setting required molecular material cell
Footpath, quality and centrifugal force, centripetal force and the parameters such as the pressure differential of different swirling turbulence main body energy fields are adjusted realizing without sieve
Separate).Coolant is taken away during produced heat energy is by equipping chuck in whole manufacture process, variety classes molecular material cell
(1 nanometer to 10 microns) manufacture of particle diameter requires to adjust coolant temperature, each rank energy field of change according to material technology
In environment temperature reach broadness (metal material, the nonmetallic materials, and disclosure satisfy that medicine of the tear of molecular material cell
Require with the harsh conditions manufacturing environment of food service industry.For inflammable and explosive simple metal material, lead in whole energy fields at different levels
The environment process for crossing vacuum or corresponding inert gas is manufactured, for special simple metal material such as titanium etc.
Adaptable humidity is kept to pack in collector).
Above specific embodiment has been described in detail to the essence of the present invention, but can not be come to the present invention's with this
Protection domain is limited.It should be evident that under the enlightenment of essence of the invention, the art those of ordinary skill can also enter
The many improvement of row and modification, it should be noted that these improve and modification all fall the present invention claims it
It is interior.